大学化学 >> 2017, Vol. 32 >> Issue (5): 55-60.doi: 10.3866/PKU.DXHX201605005

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锌配位聚合物的制备与表征——推荐一个无机化学综合实验

余凡*(),李艾华,张玉敏,邹新,胡思前   

  • 发布日期:2017-05-08
  • 通讯作者: 余凡 E-mail:yufan0714@163.com
  • 基金资助:
    湖北省武汉市教育局(2014006);国家自然科学基金(51403079)

Synthesis and Characterization of the Zinc Coordination Polymer:An Inorganic Comprehensive Experiment

Fan YU*(),Ai-Hua LI,Yu-Min ZHANG,Xin ZOU,Si-Qian HU   

  • Published:2017-05-08
  • Contact: Fan YU E-mail:yufan0714@163.com
  • Supported by:
    湖北省武汉市教育局(2014006);国家自然科学基金(51403079)

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摘要：

介绍了一个无机化学综合型新实验——锌配位聚合物的制备与表征。通过有机配体的合成、金属有机框架材料的制备及其相关结构和性能表征，使学生了解金属有机框架这一科研前沿领域，在引导学生进行实验操作、解释及归纳的过程中，提升学生的综合及创新能力。本实验综合了无机、有机和分析化学知识点的学习与实验操作能力的培养，建议纳入高年级综合型化学实验课。

关键词: 金属有机框架, 无机化学实验, 结构与性能

Abstract:

Herein, we introduce an inorganic comprehensive experiment called the synthesis and characterization of the zinc coordination polymer. The undergraduate students would know the research frontier of metal organic frameworks (MOFs) and improve the comprehensive scientific research and innovation ability during the processes of the synthesis of the organic linker, MOFs and corresponding structure-property relationship. The experiment is based on the inorganic, organic and analytical chemistry knowledge and experimental skills, which can be used as a comprehensive open experiment for senior students.

Key words: Metal organic frameworks, Inorganic chemistry experiment, Structure and properties

MSC2000: 

  • G64