University Chemistry ›› 2016, Vol. 31 ›› Issue (10): 74-79.doi: 10.3866/PKU.DXHX201601034

• Chemistry Laboratory • Previous Articles     Next Articles

Synthesis and Characterization of Macrocyclic Oxamide Complexes

Rui-Hong ZHANG*(),Guang-Ming YANG   

  • Published:2016-11-02
  • Contact: Rui-Hong ZHANG E-mail:zhangrh@nankai.edu.cn

Abstract:

Three macrocyclic oxamide complexes were synthesized by reflux and solvothermal methods.The structures were determined by X-ray crystallography.The complexes were characterized by means of elemental analyses,IR spectra,electronic spectra and ESR spectra.The experimental raw materials are simple and easy to obtain.The experimental methods are simple and easy to operate.It can train students' practical and innovative abilities.

Key words: Reflux, Solvothermal, Macrocyclic oxamide, Complex, Characterization

MSC2000: 

  • G64