微乳液法调控纳米Cu-MOF形貌的实验教学案例

doi:10.3866/PKU.DXHX202110071

Abstract

Abstract:

The morphology of Cu-MOF was controlled by microemulsion method, and the experimental condition were optimized to obtain nano Cu-MOF. In order to develop and update the teaching case for materials chemistry laboratory course, the influencing factors of experimental conditions on the morphology of Cu-MOF were explored, including cyclohexane dosage, reaction time, and reaction temperature. To meet the requirements of material chemistry laboratory course, experimental details were optimized to obtain an ideal teaching case with the advantages of good repeatability, low cost, and high feasibility. Through this experimental case, it is helpful for students to master the skills in the synthesis of nano MOFs.

Key words: Nano metal-organic framework, Microemulsion method, Morphology control, Chemistry laboratory teaching case

MSC2000:

Yinyi Liu, Zishan Su, Bixian Chen, Xin Deng, Shuru Tang, Shuman Lin, Haoyuan Xie, Xiaojun Liu, Wenting Liu, Weiqin Xu. Control the Morphology of Cu-MOF through Microemulsion Method as a Laboratory Teaching Case[J].University Chemistry, 2022, 37(7): 2110071.

Figures/Tables 5

References 24

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Control the Morphology of Cu-MOF through Microemulsion Method as a Laboratory Teaching Case

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温度/℃	时间/min	V(环己烷)/mL	形貌	尺寸	SEM
75	10	0	棱形片状	微米
75	10	10	三角形片状	纳米
75	10	16	一维棒状	纳米
35	10	10	类绣球花状	纳米
65	10	10	截面多面体	纳米