润物无声，启迪创新——从“冷冻聚合制备高分子量聚合物”综合实验谈起
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金邦坤, 何卫东
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Teaching and Learning of a Comprehensive Experiment on Synthesis of Ultrahigh Molecular Weight Polymers through Cryo-Polymerization
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Bangkun Jin, Weidong He
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表2 丙烯酰胺冷冻聚合的试剂参考用量
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| 实验序号 | AM/g a | 蒸馏水/mL | APS/mg b | TMEDA/mg b | | 1 | 0.53 (1.49) | 5.00 | 1.15 (1.00) | 1.15 (1.98) | | 2 | 0.53 (1.49) | 5.00 | 1.55 (1.35) | 1.55 (2.67) | | 3 | 0.53 (1.49) | 5.00 | 2.30 (2.00) | 2.30 (3.96) | | 4 | 0.53 (1.49) | 5.00 | 3.45 (3.00) | 3.45 (5.94) | | 5 | 0.53 (1.49) | 5.00 | 4.60 (4.00) | 4.60 (7.92) |
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