大学化学 >> 2026, Vol. 41 >> Issue (7): 290-299.doi: 10.12461/PKU.DXHX202506028

化学实验 上一篇    下一篇

室温配体辅助再沉淀法制备钙钛矿量子点及其发光性能测试的本科实验设计

于润楠, 刘熙睿, 郑翔元, 文博, 谭占鳌   

  1. 北京化工大学材料科学与工程学院, 北京 100029
  • 收稿日期:2025-06-03 录用日期:2025-07-31 发布日期:2026-06-27
  • 通讯作者: 谭占鳌 E-mail:tanzhanao@mail.buct.edu.cn Zhan'ao Tan
  • 基金资助:
    科教融汇教改项目(2024JGKJ015)

Undergraduate experimental design for preparing perovskite quantum dots via room-temperature ligand-assisted reprecipitation and investigating their luminescent properties

Runnan Yu, Xirui Liu, Xiangyuan Zheng, Bo Wen, Zhan'ao Tan   

  1. College of Materials Science and Engineering, Beijing University of Chemical Technology, Beijing 100029, China
  • Received:2025-06-03 Accepted:2025-07-31 Published:2026-06-27
  • Contact: Zhan'ao Tan E-mail:tanzhanao@mail.buct.edu.cn

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摘要： 为提升化工、化学、材料等专业本科生的科研素养与实践能力，设计了以室温配体辅助再沉淀法制备钙钛矿量子点的综合性实验，内容涵盖红光CsPbBrxI3-x和绿光CsPbBr3两种钙钛矿量子点的制备原理、合成过程、光学性能检测以及白光发光二极管的制备等。通过这一实验，让学生对钙钛矿量子点这一科学前沿具有初步了解，并在此基础上巩固无机化学、仪器分析基础知识，加深学生对溶解度、光谱分析等知识的理解，熟练掌握相关实验操作，激发对科学研究的兴趣，同时培养分析与解决实际问题的能力，为未来从事科研工作奠定坚实基础。

关键词: 钙钛矿, 量子点合成, 光致发光, 创新实验

Abstract: To improve the research literacy and practical skills of undergraduates in chemical engineering, chemistry, materials science, and related disciplines, we designed a comprehensive experiment involving the preparation of perovskite quantum dots through room-temperature ligand-assisted reprecipitation. This experiment encompasses the synthesis principles, preparation procedures, optical characterization, and fabrication of photoluminescent white light emitting diodes using both red-emitting CsPbBrxI3-x and green-emitting CsPbBr3 perovskite quantum dots. Through this experiment, students will gain fundamental knowledge about this cutting-edge research field while reinforcing their understanding of inorganic chemistry and instrumental analysis. The experiment enhances students’ comprehension of solubility principles and spectral analysis techniques, develops essential laboratory skills, stimulates scientific curiosity, and cultivates problem-solving abilities，so as to lay a solid foundation for future scientific research.

Key words: Perovskite, Synthesis of quantum dot, Photoluminescence, Innovative experiment