大学化学 >> 2023, Vol. 38 >> Issue (2): 207-213.doi: 10.3866/PKU.DXHX202206025

化学实验 上一篇    下一篇

“考古”陶片中酒类残留的分析检测

张恒1, 刘金帅1, 魏嘉遁1, 高妍2, 吴倩2, 刘刚1, 马莹1, 王芬2, 贾春江1, 苑世领1,*()   

  1. 1 山东大学化学与化工学院, 济南 250100
    2 山东大学历史与文化学院, 济南 250100
  • 收稿日期:2022-06-09 录用日期:2022-07-11 发布日期:2022-07-22
  • 通讯作者: 苑世领 E-mail:shilingyuan@sdu.edu.cn
  • 基金资助:
    教育部首批新文科研究与改革实践项目(2021100060);山东大学教育教学改革研究重点培育项目(2019P02);山东大学青年交叉科学群体项目(2020QNQT018);山东大学实验室建设与管理研究项目(sy20212202);山东大学教育教学改革研究项目(2021Y230);山东大学教育教学改革研究项目(2022Y070);山东大学教育教学改革研究项目(2022Y073)

Analysis of Alcoholic Beverage Residues in Archaeological Sherd

Heng Zhang1, Jinshuai Liu1, Jiadun Wei1, Yan Gao2, Qian Wu2, Gang Liu1, Ying Ma1, Fen Wang2, Chunjiang Jia1, Shiling Yuan1,*()   

  1. 1 School of Chemistry and Chemical Engineering, Shandong University, Jinan 250100, China
    2 School of History and Culture, Shandong University, Jinan 250100, China
  • Received:2022-06-09 Accepted:2022-07-11 Published:2022-07-22
  • Contact: Shiling Yuan E-mail:shilingyuan@sdu.edu.cn

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摘要：

通过对陶器中酒类残留的检测分析，介绍了化学技术手段在考古工作中的应用。在实验中，学生通过萃取、抽滤、离心、旋转蒸发等实验步骤提取酒的标志物——有机酸，并对其进行高效液相色谱(HPLC)检测，最后结合陶片的考古背景分析陶片的可能用途。该实验依托于考古化学这一新兴交叉学科，面向化学、考古学等专业的学生开设，有助于学生了解并掌握分析化学中样品分离和制备、液相色谱分析等基本概念与操作，并对考古学的研究内容形成一定认识。

关键词: 考古化学, 酒类残留物, 有机酸, HPLC

Abstract:

This experiment introduces the application of chemistry in archaeology through the detection and analysis of alcoholic beverage residues in pottery. Organic acids which are the indicators of alcoholic beverage residues are extracted through a series of experimental steps such as extraction, filtration, centrifugation and rotary evaporation, and measured by High Performance Liquid Chromatography (HPLC). Combined with archaeological background of pottery, the results of this experiment can be used to analyze the possible usage of the pottery. Based on emerging interdisciplinary archaeological chemistry, this experiment is offered to students majoring in chemistry and archaeology, which could provide insights into fundamental concepts, basic methods of sample isolation and HPLC analysis, as well as provide primary perception of the focused topic in archaeology.

Key words: Archaeological chemistry, Alcoholic beverage residues, Organic acid, HPLC