大学化学 >> 2025, Vol. 40 >> Issue (2): 278-288.doi: 10.12461/PKU.DXHX202405106

化学实验 上一篇    下一篇

铱配合物的合成及性质表征——一个综合化学实验

宋忠明, 马欣婷, 李抒情, 阿晟然, 张玉洋, 唐婧, 姚悦, 毛月圆, 郑胜彪, 姚湾湾   

  1. 安徽科技学院化学与材料工程学院, 安徽 蚌埠 233030
  • 收稿日期:2024-05-13 录用日期:2024-07-24 发布日期:2025-02-22
  • 通讯作者: 姚湾湾, 宋忠明 E-mail:yaoww@ahstu.edu.cn;songzhm@ahstu.edu.cn
  • 基金资助:
    安徽科技学院质量工程项目(Xj2023027,Xj2022187,Xj2023100,Xj2023041);安徽省质量工程项目(2022sykc009,2023jcjs110,2023sysx017,2023syyj040);教育部高教司协同育人项目(221000650095735)

Synthesis and Characterization of Iridium Complex: A Comprehensive Chemistry Experiment

Zhongming Song, Xingting Ma, Shuqing Li, Shengran A, Yuyang Zhang, Jing Tang, Yue Yao, Yueyuan Mao, Shengbiao Zheng, Wanwan Yao   

  1. College of Chemistry and Materials Engineering, Anhui Science and Technology University, Bengbu 233030, Anhui Province, China
  • Received:2024-05-13 Accepted:2024-07-24 Published:2025-02-22
  • Contact: Wanwan Yao, Zhongming Song E-mail:yaoww@ahstu.edu.cn;songzhm@ahstu.edu.cn

摘要: 为培养本科生的综合实践能力,本综合实验基于有机合成方法制备了一个金属有机铱配合物,探究了铱配合物的光物理性质。实验方案包括材料合成、分离提纯、结构表征、性质表征。实验内容涉及面广,知识体系较为丰富。希望能通过此实验系统锻炼学生的科研动手能力,培养学生研究有机光电功能材料的基本素质,拓宽学生的知识范围。

关键词: 铱配合物, 有机合成, 聚集诱导发光, 综合化学实验

Abstract: To enhance undergraduate students’ practical skills, this comprehensive experiment involves the synthesis of an organometallic iridium complex through organic synthesis, followed by an investigation of its photophysical properties. The experimental procedures encompass material synthesis, separation and purification, structure and property characterization. This multifaceted experiment covers a broad range of topics and provides a rich knowledge base. Our objective is to systematically develop students’ research skills, cultivate their understanding of the structure-performance relationships in organic optoelectronic materials, and broaden their academic horizons.

Key words: Iridium complex, Organic synthesis, Aggregation-induced emission, Comprehensive chemistry experiment