大学化学 >> 2025, Vol. 40 >> Issue (11): 310-317.doi: 10.12461/PKU.DXHX202503078

化学实验 上一篇    下一篇

传感技术赋能有机化学实验数字化转型——以常压蒸馏、减压蒸馏和分馏为例

吴云英1, 莫志兰1, 周雪1, 袁羽1, 马云飞1, 陈婧1, 唐刚2   

  1. 1 玉溪师范学院化学生物与环境学院, 云南 玉溪 653100;
    2 西南林业大学材料与化学工程学院, 昆明 650224
  • 收稿日期:2025-03-20 录用日期:2025-06-26 发布日期:2025-11-21
  • 通讯作者: 唐刚 E-mail:tangganghappy@163.com Gang Tang
  • 基金资助:
    云南省一流本科课程《有机化学实验》;云南省本科教育教学改革研究项目(JG2023092);云南省一流建设学科-“新学科培育计划”高原农业生态保护修复;云南省高等教育121工程项目-应用生物科学;大学生创新创业训练计划项目(S202411390012,2023A020)

Empowering the Digital Transformation of Organic Chemistry Experiments with Sensing Technology: A Case of Atmospheric Distillation, Vacuum Distillation and Fractionation

Yunying Wu1, Zhilan Mo1, Xue Zhou1, Yu Yuan1, Yunfei Ma1, Jing Chen1, Gang Tang2   

  1. 1 College of Chemistry Biology and Environment, Yuxi Normal University, Yuxi 653100, Yunnan Province, China;
    2 College of Materials and Chemical Engineering, Southwest Forestry University, Kunming 650224, China
  • Received:2025-03-20 Accepted:2025-06-26 Published:2025-11-21
  • Contact: Gang Tang E-mail:tangganghappy@163.com

摘要: 数字化实验相较于现有教材实验,具有较强的综合性、创新性和直观性。本文将数字化传感技术引入有机化学实验基本操作中,借助温度传感器和压强传感器对常压蒸馏、减压蒸馏和分馏实验开展改进与创新探索。研究结果表明,通过运用温度传感器、压强传感器对实验装置进行优化,能够实时监测常压蒸馏、减压蒸馏与分馏等基本操作过程中的温度和压强变化情况,并自动采集、记录时间–温度曲线及时间–压强曲线。这一融合举措实现了有机化学实验的数字化转变,提高了学生学习的深度与广度,可在本科有机化学实验教学中推广实施。

关键词: 温度传感器, 压强传感器, 基本操作, 实验改进, 曲线

Abstract: Compared with the experiments in existing textbooks, digital experiments are characterized by a high degree of comprehensiveness, innovativeness, and intuitiveness. This paper incorporates digital sensing technology into the basic operations of organic chemistry experiments. By means of temperature sensors and pressure sensors, explorations on the improvement and innovation of atmospheric distillation, vacuum distillation, and fractional distillation experiments are carried out. The research findings indicate that by optimizing the experimental setup with temperature sensors and pressure sensors, it is feasible to monitor in real - time the variations in temperature and pressure during fundamental operation processes such as atmospheric distillation, vacuum distillation, and fractional distillation. Moreover, the time - temperature curves and time - pressure curves can be automatically collected and recorded. This integration initiative has realized the digital transformation of organic chemistry experiments, enhanced the depth and breadth of students’ learning, and is worthy of being promoted and implemented in undergraduate organic chemistry experimental teaching.

Key words: Temperature sensor, Pressure sensor, Basic operation, Experimental improvement, Curve