大学化学综合实验三氯化六氨合钴(Ⅲ)的制备改进

doi:10.3866/PKU.DXHX201707013

Abstract

Abstract:

The experiment of hexamine cobalt(Ⅲ) chloride preparation is a comprehensive inorganic chemistry experiment, several kinds of harmful volatile reagents are used, such as concentrated hydrochloric acid, ammonia, hydrogen peroxide solution. So we explore the reaction condition to improve synthesis method. The concentration of hydrochloric acid has been decreased, the efficient value of which ranges from 3.0 mol·L^-1 to 6.0 mol·L^-1. The improvements of preparing[Co(NH₃)₆]Cl₃ are rarely reported.

Key words: Hexamine cobalt(Ⅲ) chloride, Prepare, Improvement, Hydrochloric acid concentration

Kang WANG,Jia-Bao ZHANG,Yong-Wang MA,Tong-Tong SHE,Hua TIAN,Xiao-Xia HAN. Study on the Improvement of a College Comprehensive Chemical Experiment: Preparation of Hexamine Cobalt(Ⅲ) Chloride[J].University Chemistry, 2017, 32(12): 74-78.

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Study on the Improvement of a College Comprehensive Chemical Experiment: Preparation of Hexamine Cobalt(Ⅲ) Chloride

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