大学化学 >> 2016, Vol. 31 >> Issue (12): 64-68.doi: 10.3866/PKU.DXHX201603032

化学实验 上一篇    下一篇

多孔锌MOF合成与表征的综合性无机化学实验设计

余凡*(),李艾华,张玉敏,邹新,胡思前   

  • 发布日期:2016-12-20
  • 通讯作者: 余凡 E-mail:yufan0714@163.com
  • 基金资助:
    湖北省武汉市教育局(2014006);国家自然科学基金(51403079)

An Inorganic Comprehensive Experiment Named the Synthesis and Characterization of Porous Zinc Framework

Fan YU*(),Ai-Hua LI,Yu-Min ZHANG,Xin ZOU,Si-Qian HU   

  • Published:2016-12-20
  • Contact: Fan YU E-mail:yufan0714@163.com
  • Supported by:
    湖北省武汉市教育局(2014006);国家自然科学基金(51403079)

摘要:

为将金属有机框架(MOFs)这一前沿研究领域引入本科教学实验中,特推荐一个综合性研究实验。实验内容包括有机配体的制备、MOFs材料的合成及结构和性能表征;实验技能除包含常规化学技能操作外,还包括大型仪器的学习及操作。

关键词: 金属有机框架, 结构与性能, 无机化学实验

Abstract:

A comprehensive inorganic chemistry experiment is recommended in order to introduce the frontier research field of metal organic framework to the undergraduates. The experiment contains the preparation of linker, MOFs material and corresponding characterization, while the experimental skills include the basics and the introduction and operation of large equipments for characterization.

Key words: Metal organic framework, Structure and properties, Inorganic chemistry experiment