过氧化钙制备实验的改进——以鸡蛋壳为原料

doi:10.3866/PKU.DXHX201903014

University Chemistry ›› 2019, Vol. 34 ›› Issue (9): 91-94.doi: 10.3866/PKU.DXHX201903014

• Chemistry Laboratory • Previous Articles Next Articles

Improvement of the Experiment for Synthesis of Calcium Peroxide Using Egg Shells

Min PENG,Jianxin SHI*(),Zhou WANG,Lianyun LI

School of Chemistry, Sun Yat-Sen University, Guangzhou 510275, P. R. China

Received:2019-03-08 Accepted:2019-04-08 Published:2019-04-17
Contact: Jianxin SHI E-mail:cessjx@mail.sysu.edu.cn
Supported by:
2017年中山大学校级质量工程项目“重点教材建设项目”

Abstract

Abstract:

Instead of calcium chloride, we used egg shells as material in the experiment for synthesis of calcium peroxide. This could help to improve students' environmental consciousness and stimulate students' interest in experiment. We designed procedures for egg shells pre-treatment and the synthesis of calcium peroxide, which were suitable for students. The amount of hydrogen peroxide and ammonia was optimized. The yield of anhydrous calcium peroxide was about 70% with a great than 75% purity.

Key words: Egg shell, Calcium peroxide

Min PENG,Jianxin SHI,Zhou WANG,Lianyun LI. Improvement of the Experiment for Synthesis of Calcium Peroxide Using Egg Shells[J].University Chemistry, 2019, 34(9): 91-94.

Figures/Tables 4

References 12

1	李爽; 李正阳; 马会强. 当代化工, 2015, 44 (12), 2808. doi: 10.3969/j.issn.1671-0460.2015.12.023
2	张嫦; 吴莉莉; 周小菊; 刘东. 化工环保, 2004, 24 (1), 62. doi: 10.3969/j.issn.1006-1878.2004.01.018
3	周绿山; 向文军; 唐涛; 钱跃; 王芬. 化学工程师, 2016, 250 (7), 72.
4	时运铭; 肖颖; 张萍; 刘占荣. 农业与技术, 1997, (98), 25.
5	张文昭; 张伟云. 水产养殖, 1991, (1), 26.
6	刘长虹; 吴树新. 化工科技市场, 2010, 33 (10), 21.
7	李厚金; 石建新; 邹小勇. 基础化学实验, 第2版北京: 科学出版社, 2015, 275.
8	戴小敏; 伍伟夫; 徐海燕. 大连大学学报, 2000, 12 (2), 58.
9	GeorgiaT.; 贾华敏. 中国家禽, 2007, 29 (7), 54. doi: 10.3969/j.issn.1004-6364.2007.07.022
10	陶旭; 王二雷; 张燕; 王作昭; 刘静波. 食品工业科技, 2010, (11), 382.
11	林莹; 杨军红; 田唏; 陈颖新; 李萍; 安冬; 赵文卓. 职业与健康, 2014, 30 (19), 2733.
12	钱林平; 李进之; 郑耿锋; 沈建中. 大学化学, 2018, 33 (2), 60.

编号	产品质量(m)/g	产率(Y)/%
1	1.48	40.8
2	1.04	28.7
3	1.42	39.1
4	0.97	26.7
5	1.21	33.3
6	1.84	50.7
7	1.82	50.1
8	1.62	44.6
9	1.22	33.6
10	1.71	47.1
11	1.54	42.4
12	1.39	38.3
13	1.43	39.4
14	1.82	50.1
15	1.14	31.4

编号	产品质量(m)/g	产率(Y)/%
1	2.84	78.2
2	2.71	74.7
3	3.27	90.1
4	3.06	84.3
5	3.10	85.4
6	3.55	97.8
7	2.98	82.1
8	3.00	82.6
9	2.91	80.2
10	2.85	78.5
11	2.90	79.9
12	3.35	92.3
13	2.77	76.3
14	3.30	90.9
15	3.01	82.9

测定次数	蛋壳质量(m_壳)/g	产品质量(m_产)/g	产率(Y)/%
1	7.00	3.02	75.9
2	7.02	2.74	68.8
3	7.00	2.88	72.4

测定次数	样品质量(m)/g	KMnO₄体积(V)/mL	含量(P^*)/%
1	0.0524	11.32	78.6
2	0.0590	12.48	77.0
3	0.0557	11.90	77.7

Improvement of the Experiment for Synthesis of Calcium Peroxide Using Egg Shells

RichHTML

PDF

Like

Knowledge

Abstract

Cite this article

share this article

Figures/Tables 4

References 12

Related Articles 1

Metrics

Recommended 0