Abstract: To align with the demand for cultivating students' practical and innovative capabilities under the paradigm of emerging engineering education, this study addresses the insufficient coverage of surface and interface chemistry in fundamental chemistry laboratory courses. A pedagogical framework based on the “Three-Orientation and Three-Connection” principle is proposed, establishing a systematic experimental teaching module for surface and interface chemistry. Special emphasis is placed on the strategic integration of advanced characterization techniques and corresponding curriculum design. This work provides a transferable model for the seamless incorporation of surface and interface chemistry experiments into foundational laboratory courses, demonstrating significant practical value in enhancing students' ability to employ modern analytical instrumentation to solve real-world problems, thereby fostering the development of innovative, interdisciplinary talent through the integration of scientific research and education.

Key words: Surface and interface chemistry, Experimental teaching reform, Instrument introduction, Research-education synergy, Cultivation of top-tier talents