University Chemistry ›› 2023, Vol. 38 ›› Issue (2): 221-226.doi: 10.3866/PKU.DXHX202205105
• Chemistry Laboratory • Previous Articles Next Articles
Jinshu Zhang, Yichun Wang, Jiangfeng Ni(
)
Received:2022-05-30
Accepted:2022-07-13
Published:2022-08-04
Contact:
Jiangfeng Ni
E-mail:jeffni@suda.edu.cn
Jinshu Zhang, Yichun Wang, Jiangfeng Ni. Copper Sulfide Nanoarrays for Electrochemical Copper Storage: A Recommended Comprehensive Chemical Experiment[J].University Chemistry, 2023, 38(2): 221-226.
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| 实验单元 | 具体内容 | 课时 |
| 第一单元 | 介绍铜离子电池及CuS材料的研究现状,讲解图书馆数字资源库的使用方法,介绍国内外主流学术期刊的分类,协助学生进行资料搜集、整理 | 2 |
| 第二单元 | 共同讨论学生整理的背景报告,讲解CuS纳米阵列材料的制备过程; 学生完成乙酸铜、氢氧化钠、硫化钠溶液的配制和商业碳布的亲水性处理 | 2 |
| 第三单元 | 介绍水热反应、阴离子交换反应原理及水热反应釜的使用; 学生完成CuO制备,通过阴离子交换反应最终获得CuS纳米阵列材料 | 2 |
| 第四单元 | 讲解X射线衍射仪、扫描电子显微镜、透射电子显微镜等大型仪器的原理及基础操作,带领学生观摩、完成相关的材料表征 | 2 |
| 第五单元 | 介绍扣式电池的结构及组装方法;学生完成水系铜离子扣式电池的组装 | 2 |
| 第六单元 | 讲解循环伏安法及恒流充放电测试的原理及电化学工作站、电池测试系统的使用方法: 学生完成扣式电池的电化学性能测试 | 2 |
| 第七单元 | 讲解、示范实验数据的处理和分析;学生完成实验数据的处理和分析 | 2 |
| 第八单元 | 讲解实验报告撰写要求;学生完成实验报告 | 2 |
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